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Quantitation of Acrylamide in Food Samples on the Finnigan TSQ Quantum Discovery by LC/APCI-MS/MS

the APCI source for the ionization of acrylamide from 100% water, an LOQ of 0.25 ng/mL acrylamide or 2.5 pg on column was achieved. Incorporation of a column-switching LC method prior to MS/MS detection of acrylamide eliminated the need to purify food sample extracts by SPE. Four brands of food samples were successfully analyzed for acrylamide content on the Finnigan TSQ Quantum Discovery in conjunction with the column-switching LC method.

References

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