Navigation Links
NIST releases first certified reference material for single-wall carbon nanotubes
Date:12/21/2011

The National Institute of Standards and Technology (NIST) has issued the world's first reference material for single-wall carbon nanotube soot. Distantly related to the soot in your fireplace or in a candle flame, nanotube-laden soot is the primary industrial source of single-wall carbon nanotubes, perhaps the archetype of all nanoscale materials. The new NIST material offers companies and researchers a badly needed source of uniform and well-characterized carbon nanotube soot for material comparisons, as well as chemical and toxicity analysis.

With walls of carbon only one atom thick and looking like a sheet of chicken wire curled into a cylinder, single-wall carbon nanotubes are one of several families of pure carbon materials that, because of their nanoscale size, have special properties. "Single-wall carbon nanotubes," says NIST chemical engineer Jeffery Fagan, "have exquisite optical, mechanical, thermal and electronic properties, and because of their small width but long lengthsthink of something like a long piece of hair but 10,000 times thinnerfull development of these materials should enable lighter, stronger materials, as well as improve many technologies from sensors to electronics and batteries."

Unfortunately, nanotubes are difficult to produce without significant impurities or in large quantities. Single-wall nanotubes, in particular, have been notorious for their relatively low quality and batch-to-batch variability. They typically are produced in complex processes using small particles of metal catalysts that promote the growth of the nanotubes. The resulting materialoften a powder not unlike the soot you would find in your fireplacehas frequently contained large amounts of impurities, such as other forms of carbon, and sometimes significant levels of catalysts.

"One of the issues that this reference material addresses is that there's no homogeneous lot that people can buy to do comparative measurements," says Fagan. "Even batch-to-batch, raw carbon nanotube powder samples have varied so much that there is no interlaboratory consistency. And that's particularly a problem for comparisons such as toxicity measurements. If you bought carbon nanotubes, you were pretty much guaranteed that your sample could be so different from anyone else's samples that either your measurements could be specific to some flaw of your material, or that others might not be able to reproduce what you were doing."

To address these issues, a multidisciplinary research team at NIST has worked to develop the metrology necessary for quantitative single-wall carbon nanotube measurements through a three-prong approach: basic measurement and separation science, documentary protocols and standards through international standards organizations, and now certified reference materials.

The new NIST product, Standard Reference Material (SRM) 2483, "Single-Wall Carbon Nanotubes (Raw Soot)," will directly address the issue of comparability. It is possibly the world's single largest supply of homogeneous, chemically analyzed, carbon nanotube soot where the uniformity of the samples from unit to unit is assured. Each unit of SRM 2483, a glass vial containing 250 milligrams of soot, is certified by NIST for the mass fraction values of several common contaminants: barium, cerium, chlorine, cobalt, dysprosium, europium, gadolinium, lanthanum, molybdenum and samarium. Reference values (values believed to be accurate, but not rising to the level of confidence that NIST certifies) are provided for an additional seven elements.

NIST also provides additional reference data useful for nanotube analysis, including thermal gravimetric and Raman data, as well as informational values for ultraviolet-visible-near-infrared absorbance spectra, near-infrared fluorescence spectra, Raman scattering spectra and scanning electron microscopy images. With these sets of information, purchasers of the material should be able to compare their results against the NIST values and against those from suppliers or after processing, ensuring a consistent point of comparison.


'/>"/>
Contact: Michael Baum
baum@nist.gov
301-975-2763
National Institute of Standards and Technology (NIST)
Source:Eurekalert  

Related biology news :

1. Neurotechnology Releases SentiSight 2.0 SDK Universal Object Recognition Technology
2. SNM releases new fact sheet on breast cancer and molecular imaging
3. American Dietetic Association releases 2008 nutrition trends survey
4. The International Society for Stem Cell Research releases new guidelines
5. Complete Genomics releases proof-of-concept data for its sequencing technology for the first time
6. ADA releases updated position statement on functional foods
7. DOE JGI releases expanded version of Phytozome.net
8. Afghanistan releases its first-ever list of protected species
9. ADA releases updated position paper on vegetarian diets
10. ADA releases position paper on food and water safety
11. Tackling childhood obesity at the local level -- IOM report releases Sept. 1
Post Your Comments:
*Name:
*Comment:
*Email:
Related Image:
NIST releases first certified reference material for single-wall carbon nanotubes
(Date:4/17/2017)... MELBOURNE, Florida , April 17, 2017 ... security technology company, announces the filing of its 2016 Annual Report ... Securities and Exchange Commission. ... Report on Form 10-K is available in the Investor Relations section ... well as on the SEC,s website at http://www.sec.gov . ...
(Date:4/11/2017)... Fla. , April 11, 2017 ... and secure authentication solutions, today announced that it ... Intelligence Advanced Research Projects Activity (IARPA) to develop ... Thor program. "Innovation has been a ... IARPA,s Thor program will allow us to innovate ...
(Date:4/11/2017)... MELBOURNE, Florida , April 11, 2017 ... "Company"), a security technology company, announces the appointment of independent ... John Bendheim to its Board of Directors, furthering the ... ... behalf of NXT-ID, we look forward to their guidance and ...
Breaking Biology News(10 mins):
(Date:10/11/2017)... (PRWEB) , ... October 11, 2017 , ... ... Administration (FDA) has granted orphan drug designation to SBT-100, its novel anti-STAT3 (Signal ... the treatment of osteosarcoma. SBT-100 is able to cross the cell membrane and ...
(Date:10/10/2017)... International research firm Parks Associates announced today that Tom ... 2017 Annual Meeting , October 11 in Scottsdale, Arizona ... and how smart safety and security products impact the competitive landscape. ... Parks Associates: Smart Home Devices: Main Purchase Driver ... "The residential security market has experienced continued growth, and ...
(Date:10/9/2017)... ... 2017 , ... The award-winning American Farmer television series will feature 3 Bar ... Tuesdays at 8:30aET on RFD-TV. , With global population estimates nearing ten billion ... continue to feed a growing nation. At the same time, many of our valuable ...
(Date:10/7/2017)... ... October 06, 2017 , ... Phase ... metagenome deconvolution product, featuring the first commercially available Hi-C kit. Researchers can ... Hi-C metagenome deconvolution using their own facilities, supplementing the company’s full-service ProxiMeta ...
Breaking Biology Technology: