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'Amplified' nanotubes may power the future
Date:7/14/2011

of following through when he joined the lab five years ago. "When I first heard about Rice University, it was because of Rick Smalley and carbon nanotubes," said Orbaek, a native of Ireland. "He had a large global presence with regard to nanotechnology, and that reached me.

"So I was delighted to come here and find I'd be working on nanotube growth that was related to Smalley's work."

Orbaek said he hasn't strayed far from Barron's original direction, which involved chemically attaching an iron/cobalt catalyst to the ends of nanotubes and then fine-tuning the temperature and environment in which amplification could occur.

"My group, with Smalley and Tour's group, demonstrated you could do this -- but in the first demonstration, we got only one tube to grow out of hundreds or thousands," Barron said. Subsequent experiments raised the yield, but tube growth was minimal. In other attempts, the catalyst would literally eat -- or "etch" -- the nanotubes, he said.

Refining the process has taken years, but the payoff is clear because up to 90 percent of the nanotubes in a batch can now be amplified to significant lengths, Barron said. The latest experiments focused on single-walled carbon nanotubes of various chiralities, but the researchers feel the results would be as great, and probably even better, with a batch of pristine armchairs.

The key was finding the right balance of temperatures, pressures, reaction times and catalyst ratios to promote growth and retard etching, Barron said. While initial growth took place at 1,000 degrees Celsius, the researchers found the amplification step required lowering the temperature by 200 degrees, in addition to adjusting the chemistry to maximize the yield.

"What we're getting to is that sweet spot where most of the nanotubes grow and none of them etch," Barron said.

Wade Adams, director of Rice's Richard E. Smalley Institute for Nanoscale Science and Technology and pri
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Contact: David Ruth
druth@rice.edu
713-348-6327
Rice University
Source:Eurekalert

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